Did you watch the valve operation when you were lining up TDC? The crank turns twice for every one turn of the camshaft so you could be out. Make sure that as you come up to TDC that the intake valve is open and closes as you reach TDC. When you turn past TDC the exhaust valve starts to open. Back it up to TDC and line up your distributor from there.
The second time #1 piston reachs TDC the valve operation will be the reverse. Hope this helps.
Is it cranking over fast enough? If you are trying to start an engine that also was drained of all fluids, it usually needs a little more power to crank over fast enough the first time. Try "jumping" it with another vehicle to make sure it is cranking over fast enough. What exactly is happening when you try to start it?
Benjamin
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